| Groups search result 5 for "Tobias Kind" |
Dear Jose ,
>1) which method/s are the best for the determination of nitro-PAH?
>2) Can somebody explain in deept these methods?
*1)
Depends on your available devices
with HPLC or CE : fluorescence, electrochemical, chemiluminescence
with GC-MS: chemical ionization or EI in positive or negative mode
with LC-MS: ESI, APCI in positive or negative mode
If you only have some known targets go for HPLC or LC-MS. The reduction
step to amines in HPLC may be problematic or time consuming.
If you have complex samples go for GC-MS in SIM or MS/MS mode. But also
during this analysis you need a cleanup step.
I got best results with low signal/noise ratio in MS/MS mode.
*2) I made a page with some literature with abstracts for you:
http://www.amdis.net/external/nitro-pahs.html
or try:
google and search for: "nitro PAHs" filetype:PDF
http://www.google.de/search?hl=de&q=%22nitro+PAHs%22+filetype%3APDF
*3) If you search additional publications about
3-nitro-7H-benz[d,e]anthracen-7-one (3-nitrobenzanthrone)
you can also search the Elsevier database
http://scirus.com
With kind regards
Tobias Kind
www.amdis.net
Keywords:
Nitro-PAH, Nitro-PAHs
776-34-1 1-Amino-4-nitronaphthalene 602-60-8 9-Nitroanthracene
20268-51-3 7-Nitrobenz[a]anthracene 63041-90-7 6-Nitrobenz[a]pyrene
86-00-0 2-Nitrobiphenyl 2113-58-8 3-Nitrobiphenyl
92-93-3 4-Nitrobiphenyl 7496-02-8 6-Nitrochrysene
5410-97-9 3-Nitrodibenzofuran 6639-36-7 2-Nitrodibenzothiophene
892-21-7 3-Nitrofluoranthene 86-57-7 1-Nitronaphthalene
581-89-5 2-Nitronaphthalene 17024-19-0 3-Nitrophenanthrene
82064-15-1 4-Nitrophenanthrene 954-46-1 9-Nitrophenanthrene
5522-43-0 1-Nitropyrene 33685-60-8 9,10-Dinitroanthracene
2436-96-6 2,2'-Dinitrobiphenyl N/A 2,8-Dinitrodibenzothiophene
5405-53-8 2,7-Dinitrofluorene 31551-45-8 2,7-Dinitro-9-fluorenone
606-37-1 1,3-Dinitronaphthalene 605-71-0 1,5-Dinitronaphthalene
602-38-0 1,8-Dinitronaphthalene 75321-20-9 1,3-Dinitropyrene
42397-64-8 1,6-Dinitropyrene 42397-65-9 1,8-Dinitropyrene
129-79-3 2,4,7-Trinitro-9-fluorenone 98-95-3 Nitrobenzene
88-72-2 2-Nitrotoluene 121-14-2 2,4-Dinitrotoluene
606-20-2 2,6-Dinitrotoluene 51-28-5 2-Nitrophenol
100-02-7 4-Nitrophenol 51-28-5 2,4-Dinitrophenol
88-74-4 2-Nitroaniline 99-09-2 3-Nitroaniline
100-01-6 4-Nitroaniline 534-52-1 4,6-Dinitro- o-cresol
607-57-8 2-Nitrofluorene
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